Define product and feed

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Authors: Michael Gleeson, Scumbag Sean Kelton, Thomas Considine

Contents

Introduction

A key step in the initial phases of chemical process design is the project definition. Along with the customer definition and location of the facility, the definition of the key feeds and products is important[1] (Towler, 17). Both feed and product specifications are found in the Design Basis, a non-exhaustive document containing key information and details of the plant and process.

Primary Raw Materials

The definition of raw materials on the Design Basis is located in Section 5 (see image). There are 6 main categories: Feedstock name and grade, MSDS form number, Feedstock availability, Feedstock price, Known feedstock impurities, and Additional specifications. It is of vital importance to recognize that when deciding upon feed specifications, not only stoichiometric chemistry should be considered, but also safety, yield, and environmental hazards (Biegler, 14).

Feed.png Figure 1. An example Raw Material section.

Each component of the feed, once decided upon, must be entered in the Design Basis section:

Feedstock name and grade

In this section, the the name of each component of the feed is entered. Along with the generic name of the compound, its formal chemical name, as well as grade should be included. Again, no feedstock available in industry will have 100% purity. The most common grade will be "technical" or "industrial". However, "laboratory" or "reagent" grade (higher purity) is less common.

MSDS form number

The MSDS (material safety data sheet) is an important part of dealing with any compound, with regards to operational hazards. In this section, the specific MSDS number of each component must be listed so as to be readily available in case more information is requested. MSDSs contain key physical data, such as flash point, melting point, etc.; as well as information on storage and disposal. Sources such as Perry's Chemical Engineers' Handbook also contains sources of flammability hazards of many chemicals (Seider 37).

Feedstock availability

The availability of each feedstock must also be recorded. Whether on a per year or per day basis depends primarily on the frequency of use of each specific material. This information is dependent on the overall production rate of the facility.

Feedstock price

The price of each material is listed in this sub-section. This information is highly relevant when completing the economic analysis. Note that feedstock price is highly dependent on quantity purchased. Often, the quotes of bulk chemical prices must be obtained directly from suppliers.

Known feedstock impurities

Along with the general feedstock grade (recorded in the Feedstock name and grade sub-section), the specific known impurities are recorded in this section. The name of each compound (commonly water, minerals, etc.) is recorded along with their concentrations in ppmw. The impurities are listed with the sale of the feedstock product.

Additional specifications

Any additional pertinent information about the feedstock is listed in this section. Examples include potential alternatives sources or uses.

Primary Products

The Primary Products are defined in Section 4 for the Design Basis (Please see example image below). There are 6 important subsections that must be completed within the design basis when defining the products: product name and grade, MSDS form number, production rate, product purity, product shipment mode, and additional specifications.

Each individual product that will result from the process, including wastes and side products, must be entered in the primary products section of the Design Basis.

Product Name & Grade

In this section of the design basis, the name of each product formed within the process is enter. First will be the primary desired product formed within the process followed by any side products or important waste products formed. Additionally, the desired purity (or grade) of each of these products should be specified. For example, if the product is completely pure is would be 100% grade. However, if the process creates Hydrochloric Acid in a 30% aqueous solution with water as a stabilizer, then the grade would be 30% and so on. Typically grades close to 100% are not attainable without excessive processing and thus lower grades are outputted to balance the trade-off between processing costs and purity.

MSDS Form Number

It is critical that the MSDS form be included in the design basis. The MSDS contains crucial information about the chemicals being produced including but not limited to safety/hazards information, actions to take in case of a spill/emergency, first aid measures, storage procedures, and basic material properties. This information is vital to the health of employees and safety within the plant and must be available for reference at any time throughout the design process. In order to have this information readily accessible, the MSDS form numbers should be inputted for each product in this section.

Production Rate

The mass flow rate of the products will be calculated via material balances. As an alternative, the final production rate can be obtained by looking at the output streams in the stream tables after simulating your process in specialized software (Turton p.24-25).

Product Purity

Product Shipment Mode

Additional Specifications

Case Study

As a case study, consider a plant which requires 50,000 tonnes/year of 37% formaldehyde in water (containing 8-12 wt% methanol as a stabilizer). Below is the product and feed definition of this process.

Example.jpg Product definition

Example.jpg Feed definition

Conclusion

Within the Design Basis, the definition and description of the product and feed streams is of utmost importance. Included in these sections are the names of the components, as well as their prices and key characteristics (i.e., chemical purity and grade, MSDS information, etc.). The product and feed definition is essential both in the initial and final stages of plant and process design, as it serves as a starting ground for facility design, as well as a reference of all the key components in the plant.

References

1. G.P. Towler, R. Sinnott, Chemical Engineering Design: Principles, Practice and Economics of Plant and Process Design, Elsevier, 2012.

2. L.T. Biegler, I.E. Grossmann, A.W. Westerberg, Systematic Methods of Chemical Process Design, Prentice-Hall: Upper Saddle River, 1997.

3. W.D. Sieder, J.D. Seader, D.R. Lewin, Process Design Principles: Synthesis, Analysis, and Evaluation, Wiley: New York, 2004.

4. R.T. Turton, R.C. Bailie, W.B. Whiting, J.A. Shaeiwitz, Analysis, Synthesis, and Design of Chemical Processes, Prentice Hall: Upper Saddle River, 2003.